HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzyl chloride → HCID 70620802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzyl chloride | HCID 11906 | — |
| Reactant | 4-Chlorobenzothietane-2-spiro-2'-imidazoline | HCID 70469119 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70620802 | HCID 70620802 | — |
Reaction Steps
32 Parts of 4-chlorobenzothietane-2-spiro-2'-imidazoline is reacted with 26 parts of 2-chlorobenzyl chloride in 300 parts of methanol. The yield is 52 parts (90% of theory) and the melting point is 260° C. with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04122263 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-8f40581397244e9184a7e75388e4d35a |
| Source note | uspto-grants-1978_10 |