HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22762252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 22762250 | HCID 22762250 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22762252 | HCID 22762252 | 77.5% |
Reaction Steps
A solution of 4-(4-isopropylbenzyloxy)phenyl isocyanate (4.5 g) in methylene chloride (50 ml) is added dropwise to a solution of hydroxylamine hydrochloride (5.4 g) and sodium hydroxide (4 g) in water (15 ml) at a temperature below 20° C. The reaction mixture is diluted with water and filtered to give N-[4-(4-isopropylbenzoyloxy)-phenyl]-N'-hydroxyurea (4.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04123256 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-944bcf72eaab4c1e840bface881127bf |
| Source note | uspto-grants-1978_10 |