反应详情

A mixture of 1.3g. (0.005 mole) 1-adamantyl bromomethyl ketone and 1.23g (0.005 mole) dimethyltetradecylamine was solubilized by the addition of 30cc acetone. The next day the solidified mixture was washed with ether and recrystallized from ethyl acetate to yield 2.1g white crystals, m.p. 134°-135.5°.______________________________________ Found Calculated______________________________________Carbon 67.72 67.45Hydrogen 10.65 10.51______________________________________

1. additionA mixture of 1.3g
2. washThe next day the solidified mixture was washed with ether
3. customrecrystallized from ethyl acetate