HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22762753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-(Chloromethyl)-5-(4-chlorophenyl)-1,3-oxazole | HCID 736966 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22762753 | HCID 22762753 | 71% |
Reaction Steps
A suspension of 2.3 g of 2-chloromethyl-5-(4-chlorophenyl) oxazole and 1.94 g of potassium phthalimide in 15 ml of dimethylformamide was stirred at room temperature for 1 hour. The reaction mixture was poured into 300 ml of water, and the resultant precipitate was filtered and recrystallized from ethanol to give 2.4 g (71 percent) of N-[5-(4-chlorophenyl)-2-oxazolyl]methylphthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04123541 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-8ad7817209bf4956af5e7896da38c748 |
| Source note | uspto-grants-1978_10 |