Aluminium lithium hydride → HCID 22763199, compound

Participants

Reaction Steps

The compound of Example 8 was dissolved in tetrahydrofuran and added to a suspension of lithium aluminum hydride in tetrahydrofuran and refluxed for 3 hrs. After washing with water, and extraction with ether, the subject compound was obtained; nmr (CDCl3): τ 2.25-3.15 (m, 8H, arom), 5.21 (br d, 1H, J = 5Hz, ##STR17## 5.90-6.90 (m, 5H, PhCH2 --, --OCH2 --, and --NH--), 7.25 (br t, 2H, --CH2N(CH3)2), and 7.63 (s, 6H, --N(CH3)2).

Provenance & Evidence