HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleimide → 9-(Benzyloxy)-4-[2-(2-methoxyethoxy)phenyl]pyrrolo[3,4-c]carbazole-1,3(2H,6H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleimide | HCID 10935 | — |
| Reactant | HCID 21980709 | HCID 21980709 | — |
| Product | 9-(Benzyloxy)-4-[2-(2-methoxyethoxy)phenyl]pyrrolo[3,4-c]carbazole-1,3(2H,6H)-dione | HCID 21980811 | 46% |
Reaction Steps
Reaction of (852) with maleimide using the procedure described in method 4a gave the adduct (CIII; Ar=2-(2-methoxyethoxy)phenyl, R10═H (853), which was used without further purification. Aromatisation of (853) with MnO2 using the procedure described in example 79 gave (854) (46%) as an orange solid, mp 157–159° C., which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094798B1 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-79ef9e4d9baf47909d82b5c863d6a907 |
| Source note | uspto-grants-2006_08 |