HRID11147

反应详情

EQUATION

反应方程式

HRID 11147 的结构方程式

PROCEDURE

实验过程

Reaction of (852) with maleimide using the procedure described in method 4a gave the adduct (CIII; Ar=2-(2-methoxyethoxy)phenyl, R10═H (853), which was used without further purification. Aromatisation of (853) with MnO2 using the procedure described in example 79 gave (854) (46%) as an orange solid, mp 157–159° C., which was used without further purification.

WORKUP

后处理

  1. customgave the adduct (CIII
  2. customAr=2-(2-methoxyethoxy)phenyl, R10═H (853), which was used without further purification