HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodosalicylate → Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodosalicylate | HCID 11380407 | — |
| Reactant | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| Product | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate | HCID 22000341 | 36.2% |
Reaction Steps
Following the basic procedure of Example 7(f), by reacting 5.52 g (13.4 mmol) of 7-(1-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 2.46 g (8.8 mmol) of methyl 2-hydroxy-4-iodobenzoate, 1.65 g (36%) of the expected compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723499 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-0bc171163cc04932b98554480b9c571f |
| Source note | uspto-grants-1998_03 |