Bicarbonate Ion → N-Boc-3-mesyloxypiperidine

HRID 1134492Notes

Reaction equation

HRID 1134492 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([OH:14])[CH2:11][CH2:12][CH2:13]1.[C:27](=[O:28])([O-:29])[OH:30].[CH3:15][CH2:16][N:17]([CH2:18][CH3:19])[CH2:20][CH3:21].[CH3:22][S:23]([Cl:24])(=[O:25])=[O:26].[Cl:32][CH2:33][Cl:34].[Na+:31]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([O:14][S:23]([CH3:22])(=[O:25])=[O:26])[CH2:11][CH2:12][CH2:13]1

Participants

7

Reactant 6

HCID 769Bicarbonate IonHCID 923Sodium ionHCID 6344DichloromethaneHCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 5456991-Boc-3-hydroxypiperidine

Product 1

HCID 568122N-Boc-3-mesyloxypiperidine

Sources & evidence

ORD record
ord-e4296aa8d3024284bdff4c0c89198ec3
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (7/10)

Reaction notes

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