HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 178418983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 3-(hydroxymethylidene)-1H-indol-2-one | HCID 178418741 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178418983 | HCID 178418983 | — |
Reaction Steps
E & Z 3-[(hydroxy)-methylene]-1,3-dihydro-indol-2-one is reacted with 0.022 gms. of aniline by refluxing in tetrahydrofuran (1.2 mL) for 12 hours to yield a quantitative amount (39 mg) of the named compound as a solid following concentration in vacuo, dilution with isopropanol and filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07098236B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-18311b9ff0854255a339b2693026a150 |
| Source note | uspto-grants-2006_08 |