HRID11489

反应详情

EQUATION

反应方程式

HRID 11489 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

E & Z 3-[(hydroxy)-methylene]-1,3-dihydro-indol-2-one is reacted with 0.022 gms. of aniline by refluxing in tetrahydrofuran (1.2 mL) for 12 hours to yield a quantitative amount (39 mg) of the named compound as a solid following concentration in vacuo, dilution with isopropanol and filtration.

WORKUP

后处理

  1. customto yield
  2. concentrationa quantitative amount (39 mg) of the named compound as a solid following concentration in vacuo, dilution
  3. filtrationwith isopropanol and filtration