HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20437026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Isobutyl chloroformate | HCID 62365 | — |
| Reactant | HCID 13364601 | HCID 13364601 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20437026 | HCID 20437026 | — |
Reaction Steps
A solution of 5-(4-hydroxybenzoyl)thiophene-2-sulfonamide (0.00783 mole) in acetone (50 ml) at 0° C. is treated with triethylamine (0.00861 mole) followed by isobutyl chloroformate (0.00861 mole) dropwise, during 30 minutes at 0°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04486444 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-78af13bfa7244f1daef95b5aef4bfafa |
| Source note | uspto-grants-1984_12 |