HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 178442015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-[(2-chloro-1-oxo-pentyl)-amino]-beta-oxo-N-(2-thiazolyl)-3-trifluoromethyl-benzene propanamide | HCID 13423083 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 178442015 | HCID 178442015 | — |
Reaction Steps
Using the procedure of Step B in Example 6, a mixture of 7 g of the product of Step B, 70 ml of tetrahydrofuran and 2.2 g of 4-dimethylamino-pyridine were reacted to obtain 6.1 g of 3-butyl-1,3-dihydro-1-[(2-thiazolyl)-imino]-5-trifluoromethyl-furo[3,4-b]quinoline-9-ol melting at 228° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04486438 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-2f66bc3138174480b7d2daee772596bf |
| Source note | uspto-grants-1984_12 |