HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 13075532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 2,3,3-Triiodo-2-propen-1-ol | HCID 10216731 | — |
| Product | HCID 13075532 | HCID 13075532 | — |
Reaction Steps
2.0 g of 2,3,3-triiodoallyl alcohol and 30 ml of formic acid were refluxed, with stirring, for 3 hours. After cooling the mixture, the crystals which precipitated were collected by filtration, dissolved in ethyl acetate, adsorbed in a dry silica gel chromatography column and eluted with 3:1 by volume mixture of hexane and ethyl acetate, to give 1.8 g of the desired Compound No. 81 in the form of crystals melting at 84°-85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04487781 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-9967c43190c74e3fbd834ca8706d02c5 |
| Source note | uspto-grants-1984_12 |