HRID1154015

反应详情

EQUATION

反应方程式

HRID 1154015 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

An ethanol solution of 6-[2-(1-pyrrolidinyl)ethylamino]-7,8,9,10-tetrahydro-1,2,4-triazolo[3,4-a]phthalazine was treated with an excess of ethereal hydrogen chloride. The precipitate which formed was separated by filtration to give 6-[2-(1-pyrrolidinyl)ethylamino]-7,8,9,10-tetrahydro-1,2,4-triazolo[3,4-a]phthalazine dihydrochloride melting at about 274°-275° C.

WORKUP

后处理

  1. customThe precipitate which formed
  2. customwas separated by filtration