HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4-[(4-CHLOROPHENYL)METHYL]-2,3,6,7-TETRAHYDRO-2-THIOXO-1H-IMIDAZO[1,2-a]PURIN-9(4H)-ONE MONOHYDRATE | HCID 20217703 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 178503360 | HCID 178503360 | — |
Reaction Steps
To a solution of the product of Procedure 97 (2.4 g., 0.0068 mole) in 0.1N NaOH (85 ml.), iodomethane (1.94 g., 0.0136 mole) was added and the mixture stirred at room temperature for 16 hrs. The insolubles were collected and recrystallized from methoxyethanol to give 1.3 g. of product, m.p. 296°-297°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04489078 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-05fe63d77b1c4a979b0aafcc13034709 |
| Source note | uspto-grants-1984_12 |