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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1154603Erstellt: 26. Oktober 2026

(+-)-3,4-Dimethoxyamphetamine → alpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone

https://huagongshe.com/reaction/1154603

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(+-)-3,4-DimethoxyamphetamineHCID 8423—
Edukt2-Benzyloxyphenylglyoxal hydrateHCID 20434085—
LösungsmittelDimethyl SulfoxideHCID 679—
Produktalpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenoneHCID 20434087—

Reaktionsschritte

2.3 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-3,4-dimethoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 30 minutes, whereby a solution of α-(α-methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04490392
Quelldatensatzuspto-grants-1984_12
ORD IDord-2cff76dbea424330b3a1a01aaa108953
Quellennotizuspto-grants-1984_12