HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(+-)-3,4-Dimethoxyamphetamine → alpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (+-)-3,4-Dimethoxyamphetamine | HCID 8423 | — |
| Edukt | 2-Benzyloxyphenylglyoxal hydrate | HCID 20434085 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | alpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone | HCID 20434087 | — |
Reaktionsschritte
2.3 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-3,4-dimethoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 30 minutes, whereby a solution of α-(α-methyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04490392 |
| Quelldatensatz | uspto-grants-1984_12 |
| ORD ID | ord-2cff76dbea424330b3a1a01aaa108953 |
| Quellennotiz | uspto-grants-1984_12 |