HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → 2-Methoxyphenylglyoxal hydrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | 2-Methoxy-1-phenylethanone | HCID 77698 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Methoxyphenylglyoxal hydrate | HCID 20434110 | — |
Reaction Steps
A mixture of 3 g of 2-methoxyacetophenone, 2.9 g of selenium dioxide, 20 ml of dioxane and 2 ml of water is treated in the same manner as described in Example 5-(1). 2.9 g of 2-methoxyphenylglyoxal hydrate are thereby obtained as a crude oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490392 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-daf3f1a0ab1c4380be9a35d5bce56677 |
| Source note | uspto-grants-1984_12 |