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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1154625Generated: October 25, 2026

3,4-Methylenedioxyamphetamine → alpha-(alpha-Methyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone

https://huagongshe.com/reaction/1154625

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-MethylenedioxyamphetamineHCID 1614—
Reactant2-Benzyloxyphenylglyoxal hydrateHCID 20434085—
SolventDimethyl SulfoxideHCID 679—
Productalpha-(alpha-Methyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenoneHCID 86739856—

Reaction Steps

5.2 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 15 ml of dimethylsulfoxide, and 3.54 g of α-methyl-3,4-methylenedioxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04490392
Source datasetuspto-grants-1984_12
ORD IDord-fb41cacd0f614cb9b380a237e683548b
Source noteuspto-grants-1984_12