1-Bromo-3-chloropropane → HCID 20433809, compound

HRID 1154670Notes

Reaction equation

HRID 1154670 reaction equation
[CH3:1][O:2][C:3]1[C:13]2[CH:12]=[CH:11][NH:10][C:9](=[O:14])[CH2:8][C:7]=2[C:6]([O:15][CH3:16])=[CH:5][CH:4]=1.Br[CH2:18][CH2:19][CH2:20][Cl:21]>>[CH3:1][O:2][C:3]1[C:13]2[CH:12]=[CH:11][N:10]([CH2:18][CH2:19][CH2:20][Cl:21])[C:9](=[O:14])[CH2:8][C:7]=2[C:6]([O:15][CH3:16])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 13520678HCID 13520678, compound

Product 1

HCID 20433809HCID 20433809, compound

Procedure

This compound was prepared analogous to Example 1(a) by reacting 6,9-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one (m.p. 188°-191° C.) with 1-bromo-3-chloro-propane.

Workup

  1. customThis compound was prepared analogous to Example 1(a)

Sources & evidence

ORD record
ord-6ac22271bf0c4bd9b968a2d9c92f067d
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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