1-Bromo-3-chloropropane → HCID 20433713, compound

HRID 1154671Notes

Reaction equation

HRID 1154671 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][NH:10][C:9](=[O:13])[CH2:8][C:7]=2[C:14]=1[O:15][CH3:16].Br[CH2:18][CH2:19][CH2:20][Cl:21]>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][N:10]([CH2:18][CH2:19][CH2:20][Cl:21])[C:9](=[O:13])[CH2:8][C:7]=2[C:14]=1[O:15][CH3:16]

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 20433807HCID 20433807, compound

Product 1

HCID 20433713HCID 20433713, compound

Procedure

This compound was prepared analogous to Example 1(a) by reacting 8,9-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one (m.p.: 165°-168° C.) with 1-bromo-3-chloro-propane.

Workup

  1. customThis compound was prepared analogous to Example 1(a)

Sources & evidence

ORD record
ord-62d96064e3464faba33549f783f40861
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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