Methylamine → HCID 70505503, compound

Participants

Reaction Steps

1-[3-(6-Dimethylaminomethyl-2-pyridylthio) propylamino]-1-methylthio-2-nitroethene (1.25 g, 0.0037 mol) is added to ethanol (15 ml) saturated with monomethylamine gas at ice bath temperature and is allowed to stir at ambient temperature for 18 hours. The reaction solvent is removed and the residue is chromatographed on silica gel (50 g) eluting with 5-20% methanol/chloroform to 1.1 g of a glassy product.

Provenance & Evidence