HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 12813187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12813186 | HCID 12813186 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12813187 | HCID 12813187 | — |
Reaction Steps
A 6 gram portion of 1-(4-fluorophenyl)-4-(α,α,α-trifluoro-3-tolyl)-3-pyrazolin-5-one (prepared according to the teaching outlined above) was mixed with 4 grams potassium carbonate and 15 ml. ethyl iodide in 100 ml. ethanol and refluxed overnight. The desired product was isolated in the usual way, yield 1.8 grams, m.p. approximately 92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04299614 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-c65d23e4d7fd452bae7ce5383588fa87 |
| Source note | uspto-grants-1981_11 |