HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 12813191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 2766651 | HCID 2766651 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12813191 | HCID 12813191 | — |
Reaction Steps
A mixture of 2.2 grams of the pyrazolinone prepared above, 2 grams potassium carbonate, 25 ml. ethyl iodide and 25 ml. ethanol was refluxed for about 3 hours. The reaction mixture was worked up in the usual manner to yield an oil which was identified by NMR analysis as the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04299614 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-4be818947cf04778afaacb764b9a49d1 |
| Source note | uspto-grants-1981_11 |