HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-(1,4-BENXODIOXAN-2YL)-METHYLENE-IMIDAZOLE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12761757 | HCID 12761757 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(1,4-BENXODIOXAN-2YL)-METHYLENE-IMIDAZOLE | HCID 12761756 | — |
Reaction Steps
2-(1,4-benzodioxan-2-ylmethyl)imidazole hydrochloride (1.0 g) suspended in 50 ml of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 2-(1,4-benzodioxan-2-ylmethyl)imidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04302469 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-d77029db7ac34289a69cb645ffd8aa88 |
| Source note | uspto-grants-1981_11 |