HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 13470384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 13470356 | HCID 13470356 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13470384 | HCID 13470384 | — |
Reaction Steps
1-methyl-3-methylsulphinyl-7-trifluoromethyl-4-quinolone was oxidised in dichloromethane at 0° to give 1-methyl-3-methylsulphonyl-7-trifluoromethyl-4-quinolone, m.p. 300°-301° (from methanol:ethyl acetate)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04302460 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-078ce9165c804e959b6d9a2315f94caf |
| Source note | uspto-grants-1981_11 |