HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 13022565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Fuming sulfuric acid | HCID 24681 | — |
| Reactant | N-(3-bromophenyl)-2-methylpropanamide | HCID 1234458 | — |
| Product | HCID 13022565 | HCID 13022565 | — |
Reaction Steps
Prepare a solution of 260 ml. of 30-33% oleum and 20 g. of 90% nitric acid. Cool the solution to 0° and add in small portion 60.5 g. of metabromo isobutyranilide. Maintain the reaction at 0°-5° C. for an additional 30 minutes with agitation. Isolate the product by the procedure described in Example 1 to obtain 3'-bromo-4'-nitro-isobutyranilide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04302599 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-25fcc8e93d1040b9b4d030cf363f786a |
| Source note | uspto-grants-1981_11 |