HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → N-benzylidene histidine methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | HCID 178501495 | HCID 178501495 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N-benzylidene histidine methyl ester | HCID 178501395 | — |
Reaction Steps
Histidine methyl ester, 185 mg (1 mmole), is treated with 1.06 g (1 mmole) of benzaldehyde in 25 ml of CHCl3 for 3 hours. MgSO4, 0.2 g, is added for the last hour. The mixture is filtered and the solvent is evaporated, to leaving compound 2·I as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332813 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-23d22fd2f8a342ffa48603272e1c57a8 |
| Source note | uspto-grants-1982_06 |