HRID1155675

反应详情

EQUATION

反应方程式

HRID 1155675 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Histidine methyl ester, 185 mg (1 mmole), is treated with 1.06 g (1 mmole) of benzaldehyde in 25 ml of CHCl3 for 3 hours. MgSO4, 0.2 g, is added for the last hour. The mixture is filtered and the solvent is evaporated, to leaving compound 2·I as a residue.

WORKUP

后处理

  1. filtrationThe mixture is filtered
  2. customthe solvent is evaporated
  3. customto leaving compound 2·I as a residue