HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 12900686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 12900684 | HCID 12900684 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12900686 | HCID 12900686 | 96.1% |
Reaction Steps
12.7 g of the hydrochloride of Step C in 500 ml of methanol were hydrogenated at 60° C. in the presence of 3.6 g of palladized active charcoal and the mixture was filtered. The filtrate was concentrated to dryness to obtain 9 g of 3-(1H-indol-4-yl)-3-piperidinol hydrochloride which was used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332808 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-8678530feb0d4bcfb27a6ba5ae904f0a |
| Source note | uspto-grants-1982_06 |