HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 178426987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 20537526 | HCID 20537526 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178426987 | HCID 178426987 | 19% |
Reaction Steps
In the same manner as described in Example 1-(1), 4-methyl-6-(4-dimethylaminophenyl)-2-pyridinecarboxylic acid (1.25 g), carbonyldiimidazole (1.38 g) and 5-aminotetrazole (0.47 g) are reacted to give N-(5-tetrazolyl)-4-methyl-6-(4-dimethylaminophenyl)-2-pyridinecarboxamide (0.3 g). M.P. 265°-269° C. (decomp.) (wetted from 255° C.) (recrystallized from dimethylformamide-ethanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332809 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-91d5e47bc95c419caaea3a3b9cb03b42 |
| Source note | uspto-grants-1982_06 |