HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 178463259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 20537506 | HCID 20537506 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178463259 | HCID 178463259 | 69.5% |
Reaction Steps
In the same manner as described in Example 1-(1), 4-ethoxy-6-(4-ethylaminophenyl)-2-pyridinecarboxylic acid (0.28 g), carbonyldiimidazole (0.17 g) and 5-aminotetrazole (0.09 g) are reacted to give N-(5-tetrazolyl)-4-ethoxy-6-(4-ethylaminophenyl)-2-pyridinecarboxamide (0.24 g). M.P. 255°-257° C. (decomp.) (recrystallized from dimethylformamide-ethanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332809 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-d03adf656df44b979e0d679c64b69c3a |
| Source note | uspto-grants-1982_06 |