HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178522662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-(3-Nitrophenyl)pyridine-2-carboxylic acid | HCID 12811128 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178522662 | HCID 178522662 | 96.1% |
Reaction Steps
In the same manner as described in Example 13-(1), 6-(3-nitrophenyl)-2-pyridinecarboxylic acid (4.0 g), thionyl chloride (12 ml) and 5-aminotetrazole (1.54 g) are reacted to give N-(5-tetrazolyl)-6-(3-nitrophenyl)-2-pyridinecarboxamide (4.9 g). M.P. 275°-279° C. (decomp.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332809 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-99248d2532d54b98bc8e36817c88b939 |
| Source note | uspto-grants-1982_06 |