2-Methylbutanoic Acid → HCID 20481368, compound

HRID 1155723Notes

Reaction equation

HRID 1155723 reaction equation
[CH3:1][CH:2]([CH2:6][CH3:7])[C:3]([OH:5])=[O:4].[CH3:8][S:9][CH2:10]Cl.C(N(CC)CC)C>>[CH3:1][CH:2]([CH2:6][CH3:7])[C:3]([O:5][CH2:8][S:9][CH3:10])=[O:4]

Participants

4

Reactant 3

HCID 83142-Methylbutanoic AcidHCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfide

Product 1

HCID 20481368HCID 20481368, compound

Procedure

This product was prepared according to the procedure described in Example 1, by reacting 2-methylbutyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 75°-77° C./12 mm Hg, nD20 1.4505.

Workup

  1. customThis product was prepared

Sources & evidence

ORD record
ord-e93b561eaae843b19ef207938f42d3e8
Source dataset
uspto-grants-1982_06
Patent number
US04332829

Reaction notes

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