Triethylamine → HCID 54158159, compound

HRID 1155725Notes

Reaction equation

HRID 1155725 reaction equation
[C:1]([OH:8])(=[O:7])[CH:2]=[CH:3][CH2:4][CH2:5][CH3:6].[CH3:9][S:10][CH2:11]Cl.C(N(CC)CC)C>>[C:1]([O:8][CH2:9][S:10][CH3:11])(=[O:7])[CH:2]=[CH:3][CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 144862-Hexenoic acidHCID 16916Chloromethyl methyl sulfide

Product 1

HCID 54158159HCID 54158159, compound

Procedure

This product was prepared according to the procedure described in Example 1, by reacting 2-hexenoic acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 75°-76° C./2 mm Hg, nD20 1.4836.

Workup

  1. customThis product was prepared

Sources & evidence

ORD record
ord-b83e387fc17a4b6eadba6a5fa5dd8ced
Source dataset
uspto-grants-1982_06
Patent number
US04332829

Reaction notes

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