Thionyl Chloride → HCID 11436455, compound

HRID 1155786Notes

Reaction equation

HRID 1155786 reaction equation
[C:1]([O:4][CH:5]([CH2:9][O:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:6](O)=[O:7])(=[O:3])[CH3:2].S(Cl)([Cl:19])=O>>[O:10]([CH2:9][CH:5]([O:4][C:1](=[O:3])[CH3:2])[C:6]([Cl:19])=[O:7])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 11447423HCID 11447423, compound

Product 1

HCID 11436455HCID 11436455, compound

Procedure

To 22.42 g (0.1 mole) of 2-acetoxy 3-phenoxy propanoic acid, was added 24 g of thionyl chloride and the mixture was heated under reflux for 2 hours. The excess of thionyl chloride was driven off on a rotary evaporator and the residue was distilled under nitrogen. B.P.14 =163°-8° C.

Workup

  1. temperaturethe mixture was heated
  2. temperatureunder reflux for 2 hours
  3. customThe excess of thionyl chloride was driven off on a rotary evaporator
  4. distillationthe residue was distilled under nitrogen
  5. customB.P.14 =163°-8° C.

Sources & evidence

ORD record
ord-5bc74612150c412196a06050350881aa
Source dataset
uspto-grants-1982_06
Patent number
US04332959

Reaction notes

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