HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11436455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 11447423 | HCID 11447423 | — |
| Product | HCID 11436455 | HCID 11436455 | — |
Reaction Steps
To 22.42 g (0.1 mole) of 2-acetoxy 3-phenoxy propanoic acid, was added 24 g of thionyl chloride and the mixture was heated under reflux for 2 hours. The excess of thionyl chloride was driven off on a rotary evaporator and the residue was distilled under nitrogen. B.P.14 =163°-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332959 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-5bc74612150c412196a06050350881aa |
| Source note | uspto-grants-1982_06 |