HCID 20536176, compound → HCID 20536174, compound

Participants

Reaction Steps

0.026 mol (6.5 g) of 2-acetylamino-4-nitrophenyl γ-aminopropyl ether in 32 cm3 of absolute ethanol is reduced on a 10% strength Pd/C catalyst under a hydrogen pressure of 20 bars, at 80° C., for one hour. After filtration and after cooling the filtrate with a solid carbon dioxide bath, the expected product precipitates. The product is filtered off and dried in vacuo over P2O5. It melts at 102°-106° C.

Provenance & Evidence