HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13036367, compound → HCID 13036372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13036367 | HCID 13036367 | — |
| Reactant | HCID 13036370 | HCID 13036370 | — |
| Product | HCID 13036372 | HCID 13036372 | — |
Reaction Steps
In the same manner, but replacing 4-(cycloheptimidazol-2-yl)-1-piperazinecarboxaldehyde with an equivalent amount of 4-(6-chloro-cycloheptimidazol-2-yl)-1-piperazinecarboxaldehyde, there was obtained 6-chloro-2-(1-piperazinyl)cycloheptimidazole hydrochloride: mp 210° C. (crystallized from methanol-acetone) and nmr (DMSO-d6) δ 3.30 (4H), 4.07 (4H), 7.73 (d, 2H), 8.27 (d, 2H) and 9.65 (1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04333937 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-a93d79edc1d24d6c898ecd962512f272 |
| Source note | uspto-grants-1982_06 |