HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylformamide → N-alpha-Methoxyethyl-N-ethyl-formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylformamide | HCID 12319 | — |
| Reactant | 1-Chloro-1-methoxyethane | HCID 137067 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-alpha-Methoxyethyl-N-ethyl-formamide | HCID 13684983 | — |
Reaction Steps
8.0 g of triethylamine and then a mixture of 42.5 g of triethylamine (0.5 mole in total) and 14.6 g (0.2 mole) of N-ethylformamide are added dropwise, at 0° C., to a mixture of 60 ml of light petroleum and 38 g (0.4 mole) of α-chloroethyl methyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04334097 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-2642651a432646ebae59e346fac57c31 |
| Source note | uspto-grants-1982_06 |