反应详情

A solution of 29.4 g (0.145 mole) of p-chlorophenyl vinyl sulfone in 50 ml of carbon tetrachloride at 22° was treated with 21.0 g (0.145 mole) of benzenesulfenyl chloride. There was an exotherm to 32°. The solution was removed at reduced pressure and the residue recrystallized from benzene to give product of m.p. 108.5°-109.5° C.

1. customto 32°
2. customThe solution was removed at reduced pressure
3. customthe residue recrystallized from benzene
4. customto give product of m.p. 108.5°-109.5° C.