HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → 2-CHLORO-1-(p-CHLOROPHENYLSULFONYL)ETHYL PHENYL SULFIDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | 1-Chloro-4-(ethenylsulfonyl)benzene | HCID 21703 | — |
| Reactant | Benzenesulfenyl chloride | HCID 11008040 | — |
| Product | 2-CHLORO-1-(p-CHLOROPHENYLSULFONYL)ETHYL PHENYL SULFIDE | HCID 13044795 | — |
Reaction Steps
A solution of 29.4 g (0.145 mole) of p-chlorophenyl vinyl sulfone in 50 ml of carbon tetrachloride at 22° was treated with 21.0 g (0.145 mole) of benzenesulfenyl chloride. There was an exotherm to 32°. The solution was removed at reduced pressure and the residue recrystallized from benzene to give product of m.p. 108.5°-109.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335142 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-528b65ed9c3748fea057a06f50a274a6 |
| Source note | uspto-grants-1982_06 |