HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 54367761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Benzene, (3-chloro-1-propenyl)- | HCID 94242 | — |
| Product | HCID 54367761 | HCID 54367761 | 65% |
Reaction Steps
The procedure described in Example 28 is repeated, except that 8.35 g (0.05 mol) of cinnamyl chloride and 5.4 g (0.0625 mol) of methyl acrylate are used. After a reaction time of 50 hours at 120° C., 6.10 g (0.0325 mol) of methyl 5-phenyl-2.4-pentadienecarboxylate are obtained, corresponding to a yield of 65% of theory; melting point 71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335054 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-6bdeb6f6e8024d37aeb2e8394f49b67d |
| Source note | uspto-grants-1982_06 |