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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1156469Generated: November 1, 2026

Ethylmorpholine → HCID 54377318, compound

https://huagongshe.com/reaction/1156469

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylmorpholineHCID 7525—
ReactantAcrylonitrileHCID 7855—
Reactant4-Formylbenzoyl chlorideHCID 12424620—
Catalystpalladium(II) acetateHCID 167845—
SolventP-XyleneHCID 7809—
ProductHCID 54377318HCID 54377318—

Reaction Steps

The amounts of palladium acetate shown in Table 2 below, 6.74 g (40 millimols) of 4-formylbenzoyl chloride, 2.63 ml (40 millimols) of acrylonitrile and 5.12 ml (40 millimols) of N-ethylmorpholine, in 80 ml of p-xylene, are stirred for 5 hours at 120° C. The yields of 4-formylcinnamonitrile are shown in Table 2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04335054
Source datasetuspto-grants-1982_06
ORD IDord-5d057e441cb345ca963285740d8fc5b2
Source noteuspto-grants-1982_06