HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylmorpholine → HCID 54377318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylmorpholine | HCID 7525 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 4-Formylbenzoyl chloride | HCID 12424620 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Solvent | P-Xylene | HCID 7809 | — |
| Product | HCID 54377318 | HCID 54377318 | — |
Reaction Steps
The amounts of palladium acetate shown in Table 2 below, 6.74 g (40 millimols) of 4-formylbenzoyl chloride, 2.63 ml (40 millimols) of acrylonitrile and 5.12 ml (40 millimols) of N-ethylmorpholine, in 80 ml of p-xylene, are stirred for 5 hours at 120° C. The yields of 4-formylcinnamonitrile are shown in Table 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335054 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-5d057e441cb345ca963285740d8fc5b2 |
| Source note | uspto-grants-1982_06 |