反应详情

3-(4-Biphenylyl)-3-methoxyacrylonitrile plus 3-(4-biphenylyl)-3,3-dimethoxypropionitrile (2.9 grams as a mixture from example 6), hydroxylamine hydrochloride (4.7 grams), and sodium methoxide (11.9 grams) were mixed in 500 ml. of methanol and the reaction mixture refluxed for 48 hours. The methanol was then evaporated, water added, the product separated by filtration, yield 1.2 grams.

1. customThe methanol was then evaporated
2. additionwater added
3. customthe product separated by filtration, yield 1.2 grams