HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 12960033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | — |
| Reactant | HCID 12960032 | HCID 12960032 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12960033 | HCID 12960033 | — |
Reaction Steps
5-(4-Biphenylyl)-3-aminoisoxazole (450 mg.) was mixed with excess 2,6-dichlorobenzoyl isocyanate in 50 ml. of DMF and the reaction mixture stirred overnight (about 18 hours) at room temperature. The reaction mixture was then poured into water and the product separated by filtration and recrystallized from ethanol, m.p. 225°-227° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336264 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-788a4e99153a4742b544692c5d3640db |
| Source note | uspto-grants-1982_06 |