HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl isocyanate → HCID 12960044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | — |
| Reactant | HCID 12960073 | HCID 12960073 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12960044 | HCID 12960044 | — |
Reaction Steps
5-(3-(Trifluoromethyl)phenyl)-3-aminoisoxazole (300 mg.) and excess 2,6-dichlorobenzoyl isocyanate were mixed in 50 ml. of ethyl acetate under nitrogen, and stirred for several hours at room temperature. The product was separated by filtration, m.p., 233° C. (dec)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336264 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-98c0fba7bb944708b6ed70d380580e46 |
| Source note | uspto-grants-1982_06 |