HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzoyl isocyanate → HCID 12960062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzoyl isocyanate | HCID 9942311 | — |
| Reactant | HCID 12960074 | HCID 12960074 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12960062 | HCID 12960062 | — |
Reaction Steps
5-(4-tert-Butylphenyl)-3-aminoisoxazole (1 gram) and 2 chlorobenzoyl isocyanate (1.5 ml.) were mixed in 50 ml. of ethyl acetate. The reaction mixture was stirred for 3 hours at room temperature, solvent removed, and the product separated by filtration, m.p., 213°-214° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336264 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-9405b66d13554b2289ef92bdef8c2a4e |
| Source note | uspto-grants-1982_06 |