HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12838404, compound → HCID 12838397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12838404 | HCID 12838404 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12838397 | HCID 12838397 | — |
Reaction Steps
200 g of ethyl 1-(m-methoxyphenyl)-2-oxo-cyclohexaneacetate are dissolved in 2000 ml of ethanol, and after treatment with 20 g of platinum oxide, the mixture is reduced with hydrogen at 50° C. and 50 bar. After separation of the catalyst, the solvent is removed by distillation, and there is obtained ethyl 2-hydroxy-1-(m-methoxyphenyl)-cyclohexaneacetate in the form of a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336268 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-171002af94e94b2c9bc33c333d51ce6f |
| Source note | uspto-grants-1982_06 |