Hydrochloric Acid → HCID 20534994, compound

HRID 1156567Notes

Reaction equation

HRID 1156567 reaction equation
C([NH:4][C:5]1[CH:10]=[C:9]([C:11]([CH2:17][CH3:18])([CH3:16])[CH2:12][CH2:13][CH2:14][CH3:15])[C:8]([O:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35])=[CH:7][C:6]=1[OH:36])(=O)C.[ClH:37]>C(O)C>[ClH:37].[NH2:4][C:5]1[CH:10]=[C:9]([C:11]([CH2:17][CH3:18])([CH3:16])[CH2:12][CH2:13][CH2:14][CH3:15])[C:8]([O:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35])=[CH:7][C:6]=1[OH:36]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 20534997HCID 20534997, compound

Product 1

HCID 20534994HCID 20534994, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To 6 g of 2-acetamido-4-(1-ethyl-1-methylpentyl)-5-hexadecyloxyphenol were added 30 ml of ethanol and 25 ml of concentrated hydrochloric acid, and the resulting mixture was heated on a steam bath for 4 hours. Thereafter, the reaction solution was cooled with ice whereupon it separated into two layers. The oil layer was separated and dried under reduced pressure. Yield: 3.5 g.

Workup

  1. temperaturethe resulting mixture was heated on a steam bath for 4 hours
  2. temperatureThereafter, the reaction solution was cooled with ice whereupon it
  3. customseparated into two layers
  4. customThe oil layer was separated
  5. customdried under reduced pressure

Sources & evidence

ORD record
ord-bff634cf9059413e9311d092d7e2fdf5
Source dataset
uspto-grants-1982_06
Patent number
US04336322

Reaction notes

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